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Progress in Chemistry 2022, Vol. 34 Issue (8): 1748-1759 DOI: 10.7536/PC211007 Previous Articles   Next Articles

• Review •

Catalytic Conversion of Bio-Based Platform Compounds to Fufuryl Alcohol

Qiyue Yang1, Qiaomei Wu1, Jiarong Qiu1, Xianhai Zeng2, Xing Tang2, Liangqing Zhang1()   

  1. 1 School of Advanced Manufacturing, Fuzhou University, Jinjiang 362251, China
    2 College of Energy, Xiamen University, Xiamen 361102, China
  • Received: Revised: Online: Published:
  • Contact: Liangqing Zhang
  • Supported by:
    National Natural Science Foundation of China(22108038); Tianjin University-Fuzhou University Independent Innovation Fund Cooperation Project(TF2022-10)
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Furfuryl alcohol (FOL), as an important and promising organic chemical product, can be effectively converted into various high-value chemicals, such as furfural resin, urea-formaldehyde resin, phenolic resin, fruit acid, plasticizer, rocket fuel, etc. The green FOL production by catalytic hydrogenation using furfural (FAL), xylose, and fructose as raw materials has good application prospects and research values. This article systematically reviews the research status of the FOL production from FAL, xylose, and fructose on the recent advances, and summarizes from the aspects of catalyst types, catalytic efficiency and mechanism for FOL production. On this basis, the development trends of the FOL production by catalytic hydrogenation are prospected, which may provide theoretical guidance and useful reference for developing new efficient green and stable catalytic system.

Contents

1 Introduction

2 Preparation of FOL from different substrates by catalytic conversion

2.1 Preparation of FOL from FAL by catalytic conversion

2.2 Preparation of FOL from xylose by one-pot method

2.3 Preparation of FOL from fructose by one-pot method

3 Conclusion and outlook

Key words: furfuryl alcohol, catalyst, furfural, xylose, fructose
Fig. 1 Possible reaction pathways of FAL
Fig. 2 High value-added FOL derivatives
Table 1 Preparation of FOL from FAL by noble metal catalysts
Entry Catalyst Solvent Temperature ( ℃) Time (h) Conversion (%) Selectivity (%) Run
(Stability)		 ref
1 Pt/m-CN-2 Isopropanol 70 2 98.5 99.3 5 (Stable) 37
2 Pt/(Fe, Co)-BTC-2 Isopropanol 70 2 98 99 5 (Stable) 38
3 Pt3Fe/CeO2 Isopropanol 100 4 99.8 100 6 (Stable) 39
4 Pt-0.2Co/TiO2 Methanol 50 2 100 97.5 / 40
5 0.5Pd/TiH2 Isopropanol 60 3 100 73 2 (Unstable) 41
6 Ru/Ph2P(CH2)4PPh2 / 140 1.3 >99.9 100 12 (Stable) 42
7 Ru(CO)/rGO Water 20 10 93.3 98 4 (Stable) 43
8 Au/Al2O3 / 140 / <40 100 / 32
9 Au/CeO2 / 200 / / 100 / 44
10 Ir-CoOx/A12O3 Ethanol 45 2 98 99 5 (Stable) 45
Table 2 Preparation of FOL from FAL by non-noble metal catalysts
Entry Catalyst Solvent Temperature ( ℃) Time (h) Conversion (%) Selectivity (%) Run
(Stability)		 ref
1 Cu-N/OAC 2-propanol 150 6 99.5 98.4 5 (Stable) 46
2 Cu2Zn/SiO2-IS Water 120 4 81.9 94.8 4 (Unstable) 47
3 Chi30Cu CPME 190 5 78 / / 48
4 Cu@Mg/γ-Al2O3 / 170 5 >99 94 6 (Stable) 49
5 Ni@OMC 1-propanol 180 12 92.3 98.6 5 (Stable) 50
6 C@Ni3P-1 2-propanol 160 4 97 96.3 4 (Unstable) 51
7 D-WO3 Water/Ethanol 100 2 52 85 / 54
8 CuNi/MgAlO Methanol 100 4 >99 >99 6 (Stable) 55
9 NiCoZn@CN-600 Tetrahydrofuran 160 4 100 >99 5 (Stable) 56
10 Ni-Cu Decyl alcohol 130 2 / 100 / 57
11 7Ni-Cu/ZrO2 Isopropanol 200 4 99.7 / 5 (Unstable) 58
12 2%Ni-5%Cu/SiO2 Methanol 100 2 94 64 / 59
13 CZAl Water 100 4 >99 >99 5 (Stable) 60
Table 3 Preparation of FOL using alcohols as a hydrogen donor
Entry Catalyst Solvent Temperature ( ℃) Time (h) Conversion (%) Selectivity (%) Run
(Stability)		 ref
1 6% Ru/mZrH Ethanol 150 / 92 99 / 63
2 Co-Ru/C Benzyl alcohol 150 12 98 100 4 (Stable) 67
3 10%Ni-15%W/AC Isopropanol 260 5 83 / / 68
4 Ni-SAs/NC 2-propanol 130 3 95.6 96.8 4 (Stable) 69
5 Fe-L/C-800 2-butanol 160 15 91.6 83 5 (Stable) 64
6 γ-Fe2O3@HAP Isopropanol 180 10 96.2 95.3 6 (Stable) 70
7 Fe3O4/C Isopropanol 200 4 76.4 98.5 4 (Stable) 71
8 Zr@Co-2 2-propanol 160 4 93.9 97.3 7 (Stable) 72
9 Zr5Al5 2-propanol 130 5 95 / 4 (Unstable) 65
10 CoCuAl 2-propanol 200 2 100 63 3 (Unstable) 66
11 Ov-rich meso-LMO Isopropanol 180 3 99 96 5 (Stable) 74
12 TiO2 2-pentanol 25 0.5 >99 99 2 (Stable) 75
Fig. 3 Possible reaction routes of the one-pot transformation of xylose to FOL
Table 4 Preparation of FOL from xylose
Entry Catalyst Solvent Temperature ( ℃) Time (h) Conversion (%) Selectivity (%) Run
(Stability)		 ref
1 Pt/SiO2+ZrO2-SO4 Water/2-propanol 130 6 65 51 2 (Unstable) 78
2 Pt/ZrO2-SO4 Water/Isopropanol 130 1 32 27 1 (Unstable) 79
3 Ru/MWCNT Water/2-propanol 130 6 100 9 / 80
4 Pd/MWCNT Water/2-propanol 130 6 66 12 / 80
5 Zeolite Beta Water/Isopropanol 130 1 / 75 / 81
6 [Al]-SBA-15 Water/2-propanol 130 4 13 11 3 (Unstable) 82
7 Pt/SBA-15-SO3H Water/Isopropanol 130 6 65 / 1 (Unstable) 83
8 Cu/SBA-15-SO3H Water/n-butanol 140 6 94 / / 77
9 Ru-SRGO-2 Water/1.4-dioxane 150 4 100 70.4 5 (Stable) 84
10 Cu/ZnO/Al2O3+Hβ Water/γ-butyrolactone 150 / 100 87.2 / 87
11 Formic acid+Co-N-C Water/1.4-dioxane 160 0.5 100 69.5 5 (Stable) 88
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