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Progress in Chemistry 2009, Vol. 21 Issue (12): 2718-2725 Previous Articles   Next Articles

• Review •

Analytical Technologies of Sulfur Odorants in Water with Chromatography

Li Yong**;   Zhang Xiaojian;  Chen Chao   

  1. (Department of Environmental Science and Engineering, Tsinghua University, Beijing 100084, China)
  • Received: Revised: Online: Published:
  • Contact: Li Yong E-mail:yongli05@mails.tsinghua.edu.cn
  • Supported by:

    National Natural Science Foundation of China

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Volatile organic sulfur compounds, with low odor threshold concentration and deadly toxicity, are important odorants in drinking water in China. Analytical testing techniques for sulfur odorants in water, as the foundation of all the related research, catch great attention of all. This paper reviewes the characteristics of common sulfur odorants, the main difficulties and solutions encountered in analyzing volatile organic sulfur compounds in water. A detailed discuss in selection of detector, chromatographic column, method of preconcentration in gas chromatographic determinations, which is the most practical technique among analysis of sulphur-containing compounds, and prospects of analytical testing techniques for volatile organic sulfur in water are presented in this paper.

Contents
1 Introduction
2 Common sulfur odorants in water
3 Difficulties encountered in analyzing micro amount common sulfur odorants in water
4 Analytical methods
4.1 Selection of detection system
4.2 Selection of chromatographic column
5 Preconcentration methods
5.1 Closed-loop stripping analysis
5.2 Open-loop stripping analysis
5.3 Static headspace
5.4 Purge and trap
5.5 Liquid liquid extraction
5.6 Steam distillation extraction
5.7 Solid phase extraction
5.8 Solid phase microextraction
5.9 Stir bar sorptive extraction
6 Conclusion

CLC Number: 

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