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Progress in Chemistry 2024, Vol. 36 Issue (3): 319-334 DOI: 10.7536/PC230716 Previous Articles   Next Articles

• Review •

Synthesis of Two-Dimensional Layered Zeolites and Their Catalysis, Adsorption and Separation Applications

Shiyu Hu1, Yueer Yan2(), Yahong Zhang1, Zhendong Wang3, Yi Tang1()   

  1. 1 Department of Chemistry, Fudan University, Shanghai 200438, China
    2 Institute for Preservation and Conservation of Chinese Ancient Books, Fudan University, Shanghai 200433, China
    3 State Key Laboratory of Green Chemical Engineering and Industrial Catalysis, SINOPEC Shanghai Research Institute of Petrochemical Technology Co., Ltd., Shanghai 201208
  • Received: Revised: Online: Published:
  • Contact: * e-mail: yueeryan@fudan.edu.cn (Yueer Yan); yitang@fudan.edu.cn (Yi Tang)
  • Supported by:
    National Key R&D Program of China(2018YFA0209402); National Natural Science Foundation of China(22072028); National Natural Science Foundation of China(22088101); Shanghai Natural Science Foundation(22ZR1407200)
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Compared with three-dimensional zeolites, two-dimensional layered zeolites have greater advantages in many fields, with larger surface area, shorter diffusion distance and more ductile structure. In recent years, the research on two-dimensional layered zeolites has become a new hotspot. Based on previous research and summary, this article summarizes the synthesis methods of two-dimensional zeolites in the past five years from two types of synthesis perspectives (bottom-up and top-down methods), with a focus on reviewing the progress of different synthesis methods for the same topology of zeolite. In addition, this article briefly describes the applications of two-dimensional zeolites in the fields of catalysis, adsorption, and separation and looks forward to the broad application prospects of two-dimensional zeolites so as to provide theoretical guidance and reference basis for the synthesis and application of two-dimensional zeolites.

Contents

1 Introduction

2 Synthesis of two-dimensional layered zeolites

2.1 Bottom-up synthesis method

2.2 Top-down synthesis method

3 Application of two-dimensional layered zeolite

3.1 Catalysis

3.2 Adsorption

3.3 Separation membrane

4 Conclusion and outlook

Key words: 2D zeolite, synthesis, acid catalysis, adsorption, separation membrane
Fig. 1 Zeolite frameworks approved by the IZA Structure Commission in the alphabetical order and the confirmed structures with layered forms (yellow)
Fig. 2 Schematic diagram of bottom-up synthesis of 2D zeolite
Fig. 3 Enhanced surface activity of MWW zeolite nanosheets prepared via a one-step synthesis[38]. Copyright ? 2020, American Chemical Society
Fig. 4 SEM images of MFI zeolites obtained with C22-6-6/TPAOH molar ratio of (a) 10/0, (b) 10/1, (c) 10/2, (d) 10/3, (e) 10/5, (f) 10/8, (g) 10/12, and (h) 10/20, respectively, in the dual template synthesis. (i) Commercial MFI with Si/Al ratio of ～40 was used for comparison[44]. Copyright ? 2014, American Chemical Society
Fig. 5 Schematic diagram of top-down synthesis of 2D zeolite
Fig. 6 SEM image of ITH-4 (A), ITH-10 (B), ITR-2 (C), ITR-3 (D), 0.1B-IWR-2 (E), 0.1B-IWR-6 (F), and 0.1B-IWR-2 (G)[62]. Copyright ? 2014, American Chemical Society
Fig. 7 Schematic diagram of two-dimensional zeolite vapor phase column (VPP) experiment under three-step discrete operation (a) or one-time operation conditions (b)[25] Copyright ? 2019, American Chemical Society
Fig. 8 Illustration showing the reversible swelling of MCM-22(P) and pillaring of the swollen material[72]. Copyright ? 2008, American Chemical Society
Fig. 9 SEM images of (a) 10 μm bare MFI and (b~e) BMLM particles at varying water concentrations in the synthesis [102]. Copyright ? 2012, American Chemical Society
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