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Progress in Chemistry 2022, Vol. 34 Issue (11): 2340-2350 DOI: 10.7536/PC220315 Previous Articles   Next Articles

• Review •

Progress in Circularly Polarized Light Emission of Chiral Inorganic Nanomaterials

Bin Li1,2, Ying Yu1,2, Guoxiang Xing1,2, Jinfeng Xing1, Wanxing Liu3, Tianyong Zhang1,2()   

  1. 1 Tianjin Key Laboratory of Applied Catalysis Science and Technology, School of Chemical Engineering and Technology, Tianjin University,Tianjin 300072, China
    2 Guangdong Laboratory of Chemistry and Fine Chemical Industry Jieyang Center,Jieyang 522000, China
    3 The Non-Public Enterprise Service Center of Liaocheng,Liaocheng 252000, China
  • Received: Revised: Online: Published:
  • Contact: Tianyong Zhang
  • Supported by:
    National Natural Science Foundation of China(21908161)
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Chiral inorganic nanomaterials have attracted much attention due to their excellent photophysical properties and wide potential applications. The chiral structure obtained by modifying the surface of inorganic nanomaterials with chiral ligands or assembling inorganic nanomaterials with chiral templates can strongly interact with photons to change the polarization and generate circularly polarized light (CPL). In terms of generation mechanism, CPL mainly includes circularly polarized luminescence and circularly polarized scattering, and in some cases these two mechanisms coexist. This article summarizes the progress of CPL in semiconductor nanomaterials, metal nanoclusters, perovskites, lanthanide complexes and other composite nanomaterials. In addition, the main source of CPL in different chiral inorganic nanomaterials is also discussed. The conclusions drawn in this review are expected to realize regulating the anisotropy factor of CPL active materials at the molecular level and promote their development in various applications such as quantum computing, information encryption, 3D displays, and optical sensing.

Contents

1 Introduction

2 Chiral inorganic nanomaterials with CPL

2.1 CPL from chiral inorganic semiconductor nanoparticles

2.2 CPL from chiral metal nanoclusters

2.3 CPL from chiral perovskites

2.4 CPL from chiral Lanthanide complexes

2.5 CPL from chiral nanocomposites

3 Conclusion and outlook

Key words: chirality, inorganic nanomaterials, circularly polarized light, luminescence, scattering
Fig.1 Mechanism of ligand-induced shape variations of CdSe/CdS nanostructures[35]
Fig.2 (a) TEM image and (b) CPL spectra of L/D-Au10(C13H17O5)10 nanoclusters[39]. (c) SEM image and (d) CPL spectra of Au3[(R/S)-Tol-BINAP]3Cl nanocubes in DCM containing 70% n-hexane. The inset is a side view of the nanocube[43]. (e) SEM image of right- (top) and left- (bottom) helical Ag9 nanofibers. (f) CPL spectra and gCPL distribution of chiral Ag9 nanofibers films[44]
Fig.3 CPL spectra of the chiral (a) (FMBA)2PbI4 film, (b) (ClMBA)2PbI4 film, (c) (BrMBA)2PbI4 film and (d) (IMBA)2PbI4 films[58]. R- (black line) and S- (red line). (e) Crystal structure of (S)- and (R)-3-(fluoropyrrolidinium)-MnBr3 at room temperature[59]. (f) CPL spectra of (S)- and (R)-3-(fluoropyrrolidinium)-MnBr3 at room temperature[59]
Table 1 The PLQY, magnetic transition dipole moments and |gCPL| of the chiral perovskite films[58]
PLQY
(%)		 Magnetic transition
dipole moment
(Bohr magneton)		 |gCPL|
(R-MBA)2PbI4 1.5 2.42×10-2 0.001
(S-MBA)2PbI4 1.4 2.42×10-2 0.001
(R-FMBA)2PbI4 1.0 1.17×10-2 0.0005
(S-FMBA)2PbI4 1.0 1.17×10-2 0.0005
(R-ClMBA)2PbI4 0.8 1.43×10-1 0.006
(S-ClMBA)2PbI4 0.9 1.43×10-1 0.006
(R-BrMBA)2PbI4 0.9 9.58×10-2 0.004
(S-BrMBA)2PbI4 1.0 9.58×10-2 0.004
(R-IMBA)2PbI4 0.8 6.33×10-2 0.0025
(S-IMBA)2PbI4 0.8 6.33×10-2 0.0025
Fig.4 (a) Crystal structures and (b) Temperature-dependent of circular polarized degree of chiral two-dimensional perovskites (R-MBA)2PbI4 and (S-MBA)2PbI4[51]; Magnetic field-dependent circular polarized degree of (c) rac-perovskite, (d) R-perovskite and (e) S-perovskite[60]
Fig.5 (a) Schematic diagrams and (b) CPL spectra of Eu(Ⅲ) complexes synthesized with different ligands[65]. (c) TEM image and (d) CPL spectra (λex=365 nm) of Eu3+-doped chiral TbPO4·H2O rod-like nanocrystals[66]
Fig.6 Preparation of metal-enhanced CPL-active films[69]
Fig.7 (a) Schematic diagram of the formation of gel/FeS2 helical nanofibers[73]. (b) TEM image and (c) CPL spectra of D-gel/FeS2 with P-helix and L-gel/FeS2 with M-helix nanofibers[73]. (d) SEM image and (e) CPL spectra of composite co-assembled by DGAm/CsPbX3 nanoparticles[75]
Fig.8 (a) Schematic diagram of the synthesis process of Eu2O3 and Tb2O3 nanoparticles on chiral SiO2 nanofibers[76]. (b) SEM image of nanocomposite formed by R-OPAn nanoparticles and Ag nanowires[78]. (c) CPL spectra of single R/S-OPAn nanoparticles and nanocomposite formed by R/S-OPAn nanoparticles and Ag nanowires[78]
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