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Progress in Chemistry 2021, Vol. 33 Issue (10): 1841-1855 DOI: 10.7536/PC200862 Previous Articles   Next Articles

• Review •

Preparation and Application of Poly(3,4-ethylenedioxythiophene)∶Poly(4-styrenesulfonate)/Inorganic Nanocomposites

Sha Tan1,2, Jianzhong Ma1,2(), Yan Zong1,2()   

  1. 1 College of Bioresources Chemical and Materials Engineering, Shaanxi University of Science and Technology, Xi'an 710021, China
    2 Xi'an Key Laboratory of Green Chemicals and Functional Materials, Xi'an 710021, China
  • Received: Revised: Online: Published:
  • Contact: Jianzhong Ma, Yan Zong
  • Supported by:
    National Key Research and Development Program of China(2017YFB0308602); National Natural Science Foundation of China(51903143)
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The complex of poly(3,4-ethylenedioxythiophene)∶poly(4-styrenesulfonate)(PEDOT∶PSS) is a water-soluble conducting polymer system with many advantages such as easy processability, high transmittance and flexibility. Its application, however, is only limited as flexible electrode material in some electronic devices. To solve this, introducing inorganic nanomaterials into PEDOT∶PSS complex to realize multifunctional materials is a relatively effective method to further expand its application. In this review, four most commonly used strategies to prepare PEDOT∶PSS/inorganic nanocomposites, including in-situ method, blending method, self-assembly method and intercalation method are summarized at first. Following this, each of the methods is detailed with their mechanism and experimental features, and the structural design of the nanocomposites as well as the structure-property relationships that affected by introduced inorganic nanofillers are also elucidated. Then the latest research progress of applications in sensors, solar cells, supercapacitors, thermoelectric generators of PEDOT∶PSS/inorganic nanocomposites are reviewed. Finally, the existing challenges in PEDOT∶PSS/inorganic nanocomposites studies are pointed out, and the future perspectives are provided for the research direction and potential progress and trends of these materials.

Contents

1 Introduction

2 Preparation of PEDOT∶PSS/inorganic nanocomposites

2.1 In-situ method

2.2 Blending method

2.3 Self-assembly method

2.4 Intercalation preparation method

3 Applications of PEDOT∶PSS/inorganic nanocomposites

3.1 Sensors

3.2 Solar cells

3.3 Supercapacitors

3.4 Thermoelectric generators

3.5 Other applications

4 Conclusion and outlook

Key words: PEDOT, inorganic nanomaterials, sensors, solar cells, supercapacitors, thermoelectric generators
Scheme 1 Chemical structure of PEDOT∶PSS
Fig. 1 Schematic of the fabrication of the PEDOT∶PSS-coated Cu7Te4/PEDOT∶PSS-coated Te composite film. Reprinted with permission from [38]. Copyright 2018, American Chemical Society
Fig. 2 Synthetic scheme of direct in-situ synthesis of PEDOT∶PSS/graphene/MWCNTs composites. Reprinted with permission from [55]. Copyright 2013, Royal Society of Chemistry
Fig. 3 Schematic of the preparation of PEDOT∶PSS/Au nanocomposites. Reproduced from reference [57]. Copyright 2007, American Chemical Society
Fig. 4 (a) Schematic of the preparation of Ag/PEDOT∶PSS composite interface;(b) X-ray photoelectron spectroscopy(XPS)((a) pristine PEDOT∶PSS and(b) Ag/PEDOT∶PSS);(c) transmittance spectra; and(d) ultraviolet photoelectron spectroscopy(UPS) images of pristine PEDOT∶PSS and Ag/PEDOT∶PSS films;(e) log(J)-log(V) characterization of the device with a structure of ITO/PEDOT∶PSS or Ag/PEDOT∶PSS/Ag in the dark. The doping content of Ag is 5% in volume ratio for all of the composite films. Reprinted with permission from [81]. Copyright 2019, American Chemical Society
Fig. 5 Schematic of the assembly of CoNi LDH monolayers and PEDOT∶PSS[92]. Copyright 2015, John Wiley & Sons
Fig.6 PEDOT∶PSS/iron oxide composite nanofilms transferred to various substrates:(a) freestanding PEDOT∶PSS/NP5 nanofilm(2 cm×1 cm) floating in water after PVA dissolving.(b) SEM micrographs showing PEDOT∶PSS/NP1 nanofilm collected onto a steel mesh(scale bar: 100 μm). Nanofilms collected onto(c) Teflon screw,(d) paper,(e) plastic tube, and(f) flexible PDMS. In(g), an SEM picture of the edge of ananofilm collected on paper showing the paper fiber structure to which the nanofilm conforms(scale bar: 50 μm). Reprinted with permission from [110]. Copyright 2013, American Chemical Society
Fig. 7 Inverted planar perovskite solar cell[120]
Fig. 8 Overall procedure for fabricating RuO2/PEDOT∶PSS/graphene screen-printed electrode and digital camera image of screen-printed electrode. Reprinted with permission from [123]. Copyright 2015, American Chemical Society
Fig. 9 Schematic showing the processing steps of the hybrid TE material and device: step(1), one-pot synthesis of the in situ PEDOT∶PSS/Bi2Te3 hybrid nanowire; step(2), fabrication of the self-assembled 3D network of nanowire-embedded PEDOT∶PSS nanofilms as TE test specimen; and step(3), construction of the insulator-pipeline TE device for large-scale deployment of low-temperature energetic harvesting. Reprinted with permission from [138]. Copyright 2019, American Chemical Society
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