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Progress in Chemistry 2020, Vol. 32 Issue (9): 1316-1333 DOI: 10.7536/PC200219 Previous Articles   Next Articles

• Review •

Extraction and Separation of Uranium via Solid Phase Extraction

Bo Li1,2(), Lijian Ma3,**, Ning Luo1,2, Shoujian Li3, Yunming Chen1,2, Jinsong Zhang1,2,**   

  1. 1. Nuclear Power Institute of China, Chengdu 610213, China
    2. Radioisotope Engineering Technology Research Center of Sichuan, Chengdu 610213, China
    3. College of Chemistry, Sichuan University, Chengdu 610064, China
  • Received: Revised: Online: Published:
  • Contact: Lijian Ma, Jinsong Zhang
  • Supported by:
    the National Natural Science Foundation of China(21771128, 21976125); the Nuclear Technology Application Foundaion of Nuclear Power Institute of China(16JS1807, 18JS1808)
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Uranium is an important raw material in the nuclear industry. Besides, uranium is a heavy metal with higher chemical and biological toxicity. Therefore, it is of great scientific and practical significance to efficiently separate and recover uranium from various uranium-containing aqueous systems for alleviating the shortage of uranium resources, and protecting human health and ecological environment safety. In the review, all kinds of representative solid phase extractants developed in the recent 15 years for uranium separation and recovery are briefly summarized, and the prospect and potential research directions of the solid phase extractants are also introduced.

Contents

1 Introduction

2 Solid phase extractants for uranium separation

2.1 Inorganic materials

2.2 Polymer materials

2.3 Carbonaceous materials

2.4 Metal-organic frameworks materials

2.5 Other solid phase extractants

2.6 Evaluation of the separation performance of various materials toward uranium

3 Conclusion and outlook

Key words: uranium, solid phase extraction, solid phase extractant, adsorption, separation
Fig.1 Numbers of annually published articles on the solid phase extraction of uranium in the recent 15 years(source:web of science, 2020-01 )
Fig.2 STEM-XEDS mappings of uranium reactions with hematite(Fe2O3) and nZVI at different times[5]
Fig.3 (a) Competitive adsorption of uranium on POMN in simulated seawater,(b)Water dispersion of POMN and magnetic separation[16]
Table 1 Comparison of adsorption capacity of uranium on various inorganic materials(T = 298 K)
Adsorbents pH Co(mg/L) qe(mg/g) m/v(g/L) ref
DTiOxNTs 6.0 150 366 0.2 32
CoFe2O4 6.0 300 160 1 33
IONPs 5.5 130 500 1000 39
O-Fe3O4 7.0 50 125 / 41
Fe3O4@SiO2-AO 5.0 140 105 0.4 42
QASM 3.7 60 12.5 0.77 43
EDTA-mGO 5.5 25 277 0.1 44
Fe3O4@C@Ni-Al LDH 6.0 220 174 1 45
Fe3O4@TiO2 6.0 150 90 1 46
Fe3O4/GO 5.5 50 69 0.3 48
g-C3N4/TiO2 6.9 20 64 0.25 49
Fig.4 (a) SEM images of KMS-1(left) and UO22+-exchanged KMS-1(right),(b) Mechanism of capture of UO22+ ions by KMS-1 through exchange of its interlayer potassium cations[7]
Fig.5 (a) The schematic for synthesis of MoS2-g-PDMA,(b) Possible sorption mechanism of MoS2-g-PDMA towards uranium[53]
Table 2 Comparison of adsorption capacity of uranium on various double hydroxides
Adsorbents pH Co(mg/L) qe(mg/g) m/v(g/L) ref
Cys-LDH 5.0 60 211 0.1 56
Ca/Al LDH-Gl 5.0 35 266 0.1 57
γ-Fe2O3/LDO 5.0 66 526 0.1 58
Fe3O4@C@Ni-Al LDH 6.0 220 174 1 45
LDH@nZVI 5.0 40 176 0.1 59
LDO-C 5.0 145 354 0.1 60
rGO-LDH 4.0 130 277 0.5 61
Ca-Mg-Al-LDO 5.0 70 487 0.1 62
Fig.6 Hydrated intercalation strategy synthesis of Ti3C2Tx MXene for efficient uranium separation[65]
Fig.7 Preparation of surface ion-imprinted polypropylene nonwoven fabric[87]
Fig.8 Possible sorption mechanism of CPT-T towards uranium[99]
Fig.9 (a)Synthetic procedures for COF-IHEP1,(b)experiment(black)and predicted(red)PXRD patterns of CPT-IHEP1[102]
Table 3 Comparison of adsorption capacity of uranium on various polymer materials (T = 298 K)
Adsorbents pH Co(mg/L) qe(mg/g) m/v(g/L) ref
CCTS-DHBA resin 3.0 100 330 0.2 82
PS-PAMAM-PPA 5.0 500 99.9 1 83
HSDC 4.5 250 373 0.4 84
U(Ⅵ)-ⅡP 7.0 200 134 0.5 85
ⅡP3 4.0 700 133 4 88
ⅡP 4.5 528 120 0.68
CCU 4.5 275 240 0.4 96
TCD 4.5 275 158 0.4 97
MOCOF 1 M HNO3 100 57 0.4 98
COF-IHEP1 3 120 112 0.4 102
MCPs 5.5 100 165 0.2 103
CMP-EP 6 M HNO3 100 67 1 104
PPAFs 1 250 147 0.4 105
Table 4 Comparison of adsorption capacity of uranium on various carbon materials (T = 298 K)
Adsorbents pH Co(mg/L) qe(mg/g) m/v(g/L) ref
HTC-Sal 4.3 300 261 0.5 2
HTC-Acy 4.5 300 339 0.5 114
AO-HTC-DAMN 4.3 300 466 0.4 115
HTC-btg 4.5 300 307 0.4 116
HCSs-PO4 5.0 200 286 0.2 118
AO-HTC 5.0 200 724 0.1 119
HCSs-300 7.0 50 180 0.2 120
HCC 7.0 90 273 0.2 121
AOMGO 5.0 150 286 0.2 6
AGH 6.0 250 398 0.5 130
AMGO 5.9 35 141 0.2 131
RGO-PDA/oxime 5.0 100 1049 0.001 132
CB[6]/GO/Fe3O4 5.0 75 122 0.2 133
rGO-LDH 4.0 130 277 0.5 61
FGs 5.0 250 455 0.2 134
CMK-3 6.0 120 178 0.2 137
PANI-CMK-3 6.0 120 118 0.2 138
CMK-3-SO3H 6.0 110 168 0.2 139
CMK-3-PO4 6.0 110 485 0.2 140
AO/CMK-3 6.0 110 238 0.2 141
MC-O-PO(OH)2 4.0 130 85 1 143
Oxime-CMK-5 4.5 200 65 0.4 144
P-Fe-CMK-3 4.0 300 150 0.2 145
AO-g-MWCNTs 4.5 300 145 1 149
MWNTs-C 6.0 400 89 2 150
MWNTs-F 5.0 120 72 1 131
PAMAM/WMCNT 5.0 180 80 1.5 152
MWCNTs 5.0 50 39 1 153
DGA-MWCNT / / 133 / 154
GO-CNTs 5.0 200 92 0.6 155
CoFe2O4/MWCNTs 6.0 100 213 0.4 156
PVA/MWCNTs 3.0 1000 160 0.6 157
Fig.10 Preparation of amidoxime-anchored AO-HTC-DAMN[115]
Fig.11 Proposed ligand exchange mechanism of uranyl extraction based on DFT calculation[135]
Fig.12 Preparation of ND-AO and the possible adsorption mechanism[159]
Fig.13 Synthetic route of UiO-66-AO[165]
Table 5 Comparison of adsorption capacity of uranium on various COFs (T = 298 K)
Adsorbents pH Co(mg/L) qe(mg/g) m/v(g/L) ref
MIL-101-DETA 5.5 200 350 0.4 166
ED-MIL-101(Cr) 4.5 100 200 0.5 167
MOF-AC 2 100 118 0.5 168
MOF-3 7.0 500 304 1 169
C-Zn-MOF-74 4 400 360 1 170
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GO-COOH/UiO-66 8.0 500 998 0.5 172
Fe3O4@ZIF-8 3.0 250 523 0.4 173
Fig.14 (a)and(b)Color change after MA-TMA adsorption of uranium , (c)and(d)possible coordination mechanism[180]
Fig.15 Morphology and coordination mechanism of HSOF adsorbed uranium[181]
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