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Progress in Chemistry 2020, Vol. 32 Issue (9): 1386-1401 DOI: 10.7536/PC200126 Previous Articles   Next Articles

• Review •

NiFe Layered Double Hydroxides for Oxygen Evolution Reaction

Yu Du3, Depei Liu2, Shicheng Yan1,**(), Tao Yu2, Zhigang Zou1,2   

  1. 1. National Laboratory of Solid State Microstructures, Collaborative Innovation Center of Advanced Microstructures, College of Engineering and Applied Sciences, Nanjing University, Nanjing 210093, China
    2. School of Physics, Nanjing University, Nanjing 210093, China
    3. College of Chengxian, Southeast University, Nanjing 210088, China
  • Received: Revised: Online: Published:
  • Contact: Shicheng Yan
  • Supported by:
    the National Natural Science Foundation of China(51872135, 51572121, 21603098, 21633004); the Natural Science Foundation of Jiangsu Province(BK20151265, BK20151383, BK20150580); the Fundamental Research Funds for the Central Universities(021314380133, 021314380084)
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Oxygen evolution reaction(OER) is a crucial half-reaction of energy storage and transfer technologies, such as water splitting, CO2 reduction reaction, and rechargeable metal-air batteries. NiFe layered double hydroxide(NiFe-LDH) has been considered as one of the most promising OER catalysts due to its unique layered structure, high performance, and low cost. However, it is limited by the poor conductivity and insufficient exposure to active sites. Therefore, an efficient modification method can greatly improve the electrocatalytic performance of NiFe-LDH. In this review, several typical modification methods are reviewed in detail, including defects introducing, exfoliating, elements doping, surface decorating, and in-situ growing. These methods can develop the intrinsic activity of NiFe-LDH effectively by exposing more reactive sites, increasing the conductivity, and reducing the kinetic energy barrier. Finally, the challenges and opportunities about modifications of NiFe-LDH are discussed.

Contents

1 Introduction

2 OER electrocatalysis

3 The structure of layered double hydroxides

4 Modification methods

4.1 Defect introducing

4.2 Exfoliating

4.3 Element doping

4.4 Surface decorating

4.5 In-situ growing

4.6 Other methods

5 Conclusion and prospect

Key words: NiFe-LDH, modification methods, oxygen evolution reaction, electrocatalysis
Fig.1 Catalysis mechanism of transition metal catalyst for OER[1]
Fig.2 The electron transfer steps during OER[15]
Fig.3 Schematic diagram of the structure of LDHs[7]
Table 1 Recent reports on the OER performances of modified NiFe-LDH electrocatalysts
Catalyst Currant density/mA·cm-2 Overpotential/mV Tafel slope/mV·dec-1 Main method ref
Engraved NiFe-LDH 10 250 69 Defects introducing 33
NiFe-LDH-VFe 10 245 70.0 Defects introducing 36
NiFe-LDH-VNi 10 229 62.9 Defects introducing 36
v-NiFe-LDH 10 370 - Defects introducing 37
r-NiFe-LDH 240 270 - Defects introducing 38
FeNi8Co2 LDH 10 220 42 Elements doping 39
Ni2CoⅢFe-LDH/N-GO onset 180 56.8 Elements doping & In-situ growing 40
Ni0.75Fe0.125V0.125-LDH/NF 10 231 39.4 Elements doping & In-situ growing 41
NiFeCr-6∶2∶1@CP 25 225 69 Elements doping 2
5.0%Ce-NiFe-LDH/CNT 10 227 33 Elements doping 42
NiO/NiFe-LDH 10 180 30 Surface decorating 43
NF@NiFe-LDH/CeO x 10 280 - Surface decorating & In-situ growing 44
FeOOH2nm/LDH 10 173 27 Surface decorating 45
Au/NiFe-LDH 10 237 36 Surface decorating 46
NiFe-LDH@NiCoP/NF 10 220 48.6 In-situ growing 47
NiFe-LDH/NiCo2O4/NF 50 290 53 In-situ growing 48
(Ni, Co)Se2/NiFe-LDH 10 205 61 In-situ growing 49
NiFe-LDH-NS 10 300 40 Exfoliating 11
PM-NiFe-LDH 10 230 47 Exfoliating 50
NiFe-LDH-UF 10 254 32 Exfoliating 51
NiFe-LDH-NS@DG 10 10 210 52 Exfoliating & In-situ growing 52
NiFe-LDH/RGO 30 273 49 Exfoliating & In-situ growing 53
Fig.4 (a) Schematic illustration of defective NiFe-LDH with oxygen vacancies prepared by fast reducing flame treatment,(b) LSV curves,(c) chronoamperometry curves, SEM of flame-engraved NiFe-LDH(d) before and(e) after stability test[33]
Fig.5
Fig.6 Schematic diagram of the synthesis of v-NiFe LDH with metal ions and oxygen vacancies[37]
Fig.7 (a) Schematic representation of exfoliation of NiFe-LDH,(b) Chronoamperometric measurement with Overpotential at 300 mV,(c) LSV curves[11]
Fig.8 The morphology of (a) porous monolayered NiFe-LDH[50] and (b) sub-3 nm ultrafine monolayered NiFe-LDH[51]
Fig.9 (a) LSV curves and(b) EIS curves with different Ni/Co ratios[39]
Fig.10 (a) Schematic illustration of fabrication process and crystal structure of preoxidized trinary LDH,(b, c) TEM images of NiCoFe-LDH and O-NiCoFe-LDH nanoplate.[71]
Fig.11 OER performance of NiO/NiFe-LDH,(a)LSV curves,(b)Tafel curves,(c) Comparison on the overpotentials at 10 mA·cm-2 and Tafel slopes of recently reported earth-abundant OER catalysts,(d) the chronopotentiometric curve of NiO/NiFe-LDH[43]
Fig.12 (a) TEM,(b) HAADF-STEM and(c) EDS mapping images of sAu/NiFe LDH.(d) Au L3-edge XANES spectra of the experimental and simulated results for sAu/NiFe LDH, and the Au foil.(e) Differential charge densities of NiFe LDH with and without Au atom when one O atom is adsorbed on the Fe site. The iso-surface value is 0.004 e?-3. Yellow and blue contours represent electron accumulation and depletion, respectively[46]
Fig.13 Schematic representation of the synthesis of 3D hierarchical NiFe-LDH@NiCoP/NF electrodes[47]
Fig.14 TEM image and schematic diagram of NiFe-LDH HMS[104]
Table 2 Pros and cons of various modification methods
Methods Advantages Disadvantages
Defect introducing Tuning electronic structure with the formation of edge, corner and defect sites Aggregation
Exfoliating Increasing the exposure of active sites Aggregation
Element doping Regulating the electronic structures and enhancing the intrinsic catalytic activity Limited improvement in catalytic performance
Surface decorating Changing intrinsic electronic structure A limited number of active sites
In-situ growing Preventing aggregation and the synergistic effect to enhance OER stability and activity Limited amount of loading scales
Fig.15 Schematic representation of NiFe-LDH/GO’s structure and its OER activity[53]
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