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Progress in Chemistry 2019, Vol. 31 Issue (2/3): 442-454 DOI: 10.7536/PC180714 Previous Articles   Next Articles

Rich-Nickel Ternary Layered Oxide LiNi0.8Co0.1Mn0.1O2 Cathode Material

Ze Feng, Dan Sun, Yougen Tang**(), Haiyan Wang**()   

  1. Hunan Provincial Key Laboratory of Chemical Power Sources, Hunan Provincial Key Laboratory of Efficient and Clean Utilization of Manganese Resources, College of Chemistry and Chemical Engineering, Central South University, Changsha 410083,China
  • Received: Online: Published:
  • Contact: Yougen Tang, Haiyan Wang
  • About author:
    ** E-mail: (Yougen Tang);
    (Haiyan Wang)
  • Supported by:
    National Key R&D Program of China(2018YFB0104000); Science and Technology Major Project of Hunan Province(2017GK1040); Science and Technology Major Project of Hunan Province(2017GK5040); Science and Technology Plan Project of Hunan Province(2016TP1007); Science and Technology Plan Project of Hunan Province(2017TP1001); Innovation-Driven Project of Central South University(2016CXS009)
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Nickel-rich ternary layered oxide LiNi0.8Co0.1Mn0.1O2 (NCM811) is considered to be one of the most potential cathode materials in the next generation lithium-ion batteries due to its high reversible capacity, environmentally friendly feature and low cost. However, this kind of cathode material is suffering from the poor thermal stability, phase transition during the charge-discharge process and safety issue, which hinders its further practical application. With the deepening of researches and development of fabrication methods, the electrochemical properties of NCM811 have been significantly improved. In this paper, the recent research progress of nickel-rich layered oxide NCM811 cathode material has been reviewed. We mainly focus on the problems and declined mechanisms, synthesis methods, improvement measures and theoretical calculation simulation studies of NCM811, and also make a brief outlook for the future development of nickel-rich ternary layered oxide NCM811.

Key words: LiNi0.8Co0.1Mn0.1O2, phase transition, preparation method, simulation
Table 1 Main performance parameters of commercial cathode materials[7,8,9]
Parameter LiMn2O4 LiFePO4 LiCoO2 LiNixCoyMzO2
Crystal structure Spinel Olivine Layered Layered
Theoretical capacity(mAh·g-1) 148 170 274 278
Test capacity(mAh·g-1) 90~120 110~160 140~170 145~200
Operating Voltage(V) 3.8 3.5 3.7 3.6
Raw materials Abundant Abundant Lacking Sufficient
Fig. 1 Cation mixing of different regions in nickel-rich ternary cathode material[14]
Fig. 2 Schematic diagram of phase transitions in ternary material structures results from in situ TR-XRD with MS analysis[19]
Table 2 The results of characterization and calculation in anode after 3000 cycles[57]
Sample Estimated SEI thickness by XPS(nm) Calculated weight of Li in LiF as SEI(mg) Calculated capacity loss by Li in SEI(mAh) Estimated anode potential after capacity Loss(V)
Cell-Mo after 3000 cycles 10 2.65 10.2 0.56
Cell-Ref after 3000 cycles 20 5.30 20.4 0.63
Fig. 3 Synthesis process of LixAlO2 and LixTi2O4 coating layers on NCM811 cathode[71]
Fig. 4 Spherical gradient nickel-rich material[17]
Fig. 5 Formation model of SEI layer in polycrystalline and single crystal cathode materials[78]
Fig. 6 Synthesis of single crystal NCM811 material under different fluxes and temperatures[43]
Fig. 7 The structures of the different additives(a) and their linear volt-ampere scanning curves(b)[90]
Fig. 8 The bond strength between different transition metals[16]
Fig. 9 The formation energy of defective sites for structures of un-doped, Al-and Mg-doped in the case of(a) the oxygen vacancy(VO),(b) excess Ni(Ni Li), and(c) Li/Ni exchange(LiNi-NiLi)[96]
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