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Progress in Chemistry 2020, Vol. 32 Issue (12): 2049-2063 DOI: 10.7536/PC200404 Previous Articles   Next Articles

• Review •

Morphology Control of Layered Double Hydroxide and Its Application in Water Remediation

Weiyang Lv1,**(), Ji’an Sun1, Yuyuan Yao1, Miao Du2, Qiang Zheng2   

  1. 1 School of Materials Science and Engineering, Zhejiang Sci-Tech University, Hangzhou 310018, China
    2 Department of Polymer Science and Engineering, Zhejiang University, Hangzhou 310058, China
  • Received: Revised: Online: Published:
  • Contact: Weiyang Lv
  • Supported by:
    the National Natural Science Foundation of China(No. 51873180); the National Natural Science Foundation of China(51973183)
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As a typical representative of inorganic layered materials, layered double hydroxide(LDH) has attracted intensive interest in the well-established and advanced fields of applications. However, current studies on the function optimization of LDH mainly focus on tuning the composition, interlayer anions and particle size, ignoring the relationship between the morphology and property. This review starts with a brief introduction of the basic structure and property of LDH, and then summarizes the LDH synthetic methods of the traditional hexagonal platelets and novel morphologies like microspheres, nanocages, nanowires and nanorings. To improve the comprehensive performance of LDH composite materials, the construction mechanism has been deeply explored through controlling the reaction condition and formulation, as well as the surface property of matrix. In addition, we also discuss the potential applications of LDH composites in water remediation as the adsorbents, catalysts and separation materials. Finally, the present difficulties and development trends of controlling synthesis of LDH are prospected.

Contents

1 Introduction

2 Basic structure and property of LDH

2.1 Composition and structure of LDH

2.2 Characteristic property of LDH

3 Preparation methods of LDH

3.1 Synthesis of LDH with traditional morphology

3.2 Synthesis of LDH with novel morphology

4 Controllable preparation of LDH composites

4.1 Effect of reaction formulation

4.2 Effect of reaction condition

4.3 Effect of surface property

5 Water remediation by LDH materials

5.1 Adsorbents

5.2 Catalysts

5.3 Separation materials

6 Conclusion and outlook

Key words: layered double hydroxide, preparation methods, morphology control, composite materials, water remediation
Fig.1 Schematic representation of the structure of LDH, the general elemental composition is also indicated[18]
Fig.2 (a~d) Illustrations of the crystal structure and the screw dislocation-driven growth of 2D LDH into nanoplates and nanoflowers,(e, f) SEM images of LDH with different magnifications,(g, h) tapping mode AFM images of LDH[57]
Fig.3 TEM and SEM images of LDH synthesized by sacrificial template method with different morphologies: (a) core-shell microspheres[85],(b) yolk-shell microspheres[85],(c) hollow microspheres[85],(d) nanocages with MOF inside[93],(e) hollow nanocages[93],(f) hollow prism[94],(g) hollow nanospheres[97],(h) 3 D ordered microporous structure[98] and (i) nanowires[99]
Fig.4 TEM images of LDH synthesized by soft template method with different morphologies: (a) belt-like structure[100],(b) nanorods[100],(c) rope-like structure[107],(d) core-shell microspheres[108],(e) yolk-shell microspheres[108],(f) hollow microspheres[108],(g, h) nanoscrolls and (i) nanosheets[109]
Fig.5 TEM images of the CoAl-LDH at different reaction times: (a) 0.5 h,(b) 1 h,(c) 1.5 h,(d) 2 h,(e) 2.5 h and (f) 3 h.(g) The size distributions of both nanosheet and nanoring at different reaction times[112]
Fig.6 SEM images of PVDF@LDH composite fibrous membranes synthesized by (a) MgAl(NO 3) and (b) MgAl(SO 4), (c) Schematic illustration of the growth mechanism of LDH on PVDF nanofiber surface[122]
Fig.7 SEM images of the LDH grown on the modified SiO 2nanofibers at different reaction times: (a) 3 h,(b) 6 h,(c) 12 h and (d) 24 h[126]
Table 1 The performance comparison of LDH with different morphologies in water treatment
Application Sample Metbod Morphology Pollutant Property ref
Adsorbents CoAl-LDH Surfasctant template Nanoscrolls Mecthyl orange 1153.94 mg/g 109
(Capacity) Coprecipitation Nanosheets 347.11 mgg
MgAl-LDH Surfisctant template Foum-like Bromate 59.34 mg/g 113
Coprecipitation Platc-like 16.36 mgg
ZnAl-LDO Sarificial template Hollow spheres Orange II 849.7 mg/g 173
Coprecipitation Plate-like 676.1 mg/g 174
CaAl-LDH Solvothermal Nanorods Unanium 266.5 mg/g 175
Coprecipitation Plate-like 54.8 mg/g 176
Catalysts ZnTi-LDH Sufuctant template Particles arangement Mecthyl orange 95.4% 158
(Removal rate) Hydrothermnal Sheet-like 71.0%
NiFe-LDH Hydrothermal Spheres Methylene blue 67.87%(COD) 177
Coprecipitation Sheet-like 58.96%(COD)
Separation materials NiCo-LDH/PVDF Hydrothermal(6h) Grass-like Peroleum ether ~ 690 Lm-2·h-1 170
(Flux) Hydrothermal(3h) Nanosleets ~590 Lm -2·h -1
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