• Review •
Xuemei Wei, Zhanwei Ma, Xinyuan Mu, Jinzhi Lu, Bin Hu. Catalyst in Acetylene Carbonylation: From Homogeneous to Heterogeneous[J]. Progress in Chemistry, 2021, 33(2): 243-253.
Entry | Catalyst | T (℃) | P (MPa) | Yield (%) | ref |
---|---|---|---|---|---|
1 | Pd/Cl2 | 100 | 9.8 | 38.5 | |
2 | Pd(OAc)2-diphenyl-2- pyridylphosphine | 50 | 5 | 85.0 | |
3 | PdCl2-HgCl2 | -20 | 0.1 | 96.0 | |
4 | PdCl2-SnCl2 | r.t | > 0.1 | 100 | |
5 | PdCl2-thiourea | 20 | 0.1 | 90 | |
6 | PdCl2/CuCl2/ HCl/O2 | r.t | 0.1 | Eq. | |
7 | PdCl2/FeCl3/ H2SO4/O2 | 35 | 0.004 | 47.8 | |
8 | PdI2/KI/Air | 60 | 3.0 | 92 | |
9 | Pd(OAc)2/HQ-Cl/ NPMoV/O2 | 25 | 0.1 | 85 | |
10 | Pd(xantphos)Cl2 | 25 | 0.1 | 97 | |
11 | PdX2-HY-Ox-O2 | 25 | 0.1 | 100 | |
12 | PdBr2-LiBr | 25 | 0.1 | 94.9 |
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