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化学进展 2019, Vol. 31 Issue (9): 1283-1292 DOI: 10.7536/PC190219 前一篇   后一篇

• •

MXene及其复合材料在钠/钾离子电池中的应用

李佳慧1,2, 张晶1,2, 芮秉龙1,2, 林丽1,2, 常立民1,2,**(), 聂平1,2,**()   

  1. 1. 吉林师范大学环境友好材料制备与应用教育部重点实验室 长春 130103
    2. 吉林师范大学化学学院 四平 136000
  • 收稿日期:2019-02-21 出版日期:2019-09-15 发布日期:2019-07-02
  • 通讯作者: 常立民, 聂平
  • 基金资助:
    国家重点研发计划(No.SQ2017YFGH001474); 国家自然科学基金项目(No.51802111); 国家自然科学基金项目(No.51778268); 吉林省自然科学基金项目(No.20180101192JC); 吉林省“十三五”科学技术项目以及吉林师范大学科研项目(No.JJKH20190997KJ)
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Application of MXene and Its Composites in Sodium/Potassium Ion Batteries

Jiahui Li1,2, Jing Zhang1,2, Binglong Rui1,2, Li Lin1,2, Limin Chang1,2,**(), Ping Nie1,2,**()   

  1. 1. Key Laboratory of Preparation and Applications of Environmental Friendly Materials of the Ministry of Education, Jilin Normal University, Changchun 130103, China
    2. College of Chemistry, Jilin Normal University, Siping 136000, China
  • Received:2019-02-21 Online:2019-09-15 Published:2019-07-02
  • Contact: Limin Chang, Ping Nie
  • About author:
    ** E-mail: (Limin Chang)
    (Ping Nie)
  • Supported by:
    The National Key R&D Program of China(No.SQ2017YFGH001474); The National Natural Science Foundation of China(No.51802111); The National Natural Science Foundation of China(No.51778268); The Natural Science Foundation of Jilin Province(No.20180101192JC); The Funding of Research Program of Jilin Normal University(No.JJKH20190997KJ)

MXene作为一种新型的二维层状结构材料而备受关注, MXene具有高电子传导率、较大的比面积、较好的机械性能以及独特的层状结构, 已广泛应用于储能、催化、吸附等领域。近年来, MXene及其复合材料应用于二次电池领域引起了人们的广泛关注。氧化物、硫化物等材料具有高容量, 但存在电导率低、反应过程中体积膨胀、循环稳定性差等问题, 构建与MXene的复合材料既能提高容量又可以增强材料的电子导电率, 有效缓解反应过程中体积膨胀, 实现最佳的电化学性能。本文主要对MXene及其复合材料在钠离子电池和钾离子电池中的最新研究进展进行总结, 简要介绍了钠离子电池、钾离子电池和MXene的研究背景, 重点介绍了MXene复合材料在钠离子电池中的应用研究, 主要按照硫化物、氧化物、碳材料进行分类, 对其合成方法与电化学性能进行综述, 同时总结了MXene复合材料在钾离子电池中的研究进展。最后本文对MXene及其复合材料的发展及其应用前景进行了总结与展望。

关键词： MXene, 钠离子电池, 钾离子电池, 负极, 复合材料

MXene has attracted considerable attention as a new type of two-dimensional layered structural materials owing to its high electron conductivity, large specific area, excellent mechanical properties and unique layered structure, which make it promising for application in energy storage, catalysis and adsorption. MXene and its composites have recently aroused intense interest for rechargeable batteries. Transition metal sulfides and oxides have the merits of high capacity, however suffering from issues of low conductivity, relatively large volume expansion and poor capacity retention during cycling. Combining MXene with these materials can not only increase the specific capacity, but also enhance electronic conductivity and solve the volume change during electrochemical cycling, finally achieving superior electrochemical properties. This review covers the key technological developments and latest progress of MXene composites in sodium ion batteries and potassium ion batteries. Starting from a brief introduction of the background of sodium ion batteries, potassium ion batteries and MXene, we mainly focus on research progress on synthesis and application in sodium ion batteries, including sulfides, oxides, and carbonaceous materials. The study on potassium ion batteries is still in its infancy. Current status of MXene and its composite in potassium ion batteries have also been summarized, also current challenges and future perspectives in the application of MXene materials are discussed.

Key words: MXene, sodium ion batteries, potassium ion batteries, anode, composites
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图1 2013~2018年Web of Science上检索主题词为“MXene”和“batteries”的论文数量(检索时间:2019年1月)
Fig. 1 The number of published papers from Web of Science(Search time:Jan. 2019) with topics “MXene” and “batteries” from 2013 to 2018
图2 MAX相剥离过程和MXenes制备的示意图[17]
Fig. 2 Schematic for the exfoliation process of MAX phases and formation of MXenes[17].Copyright 2012, American Chemical Society
图3 (a)MAX的结构和相应的MXenes示意图[18];(b)HF处理后的Ti3AlC2(Ti3C2Tx)的扫描电子显微镜图像[17]
Fig. 3 (a) Structure of MAX phases and the corresponding MXenes[18];(b) SEM image for Ti3AlC2 after HF treatment(Ti3C2Tx)[17].Copyright 2014, Wiley-VCH; Copyright 2012, American Chemical Society
图4 (a)使用MOH制备M’-c-Ti3C2Tx(M+=Li +, Na +, K+, TBA+)的工艺示意图;(b)Na-c-Ti3C2Tx的扫描电子显微镜图像, 插图显示更高放大倍率的图像;(c)高分辨透射电子显微镜图像显示堆叠的层[49]
Fig. 4 (a) Schematic of fabrication process for M’-c-Ti3C2Tx(M+=Li +, Na +, K+, TBA+)by flocculation using MOH;(b) SEM image of Na-c-Ti3C2Tx flocculated networks. Inset shows a higher magnification image;(c) HRTEM image showing stacked layers[49]. Copyright 2018, The Royal Society of Chemistry
图5 (a)真空抽滤制备MXene/SnS2复合材料的示意图;(b)MXene/SnS2-5∶1的扫描电子显微镜图像;(c, d)CoS/MXene的高分辨率透射电子显微镜图像;(e)CoS/MXene复合材料合成工艺示意图;(f)MXene/SnS2 10∶1, MXene/SnS2 5∶1, MXene/SnS2 2∶1和MXene的循环性能;(g)不同电流密度下CoS/MXene的倍率性能[43, 44]
Fig. 5 (a) Schematic illustration of the preparation of MXene/SnS2 composite by vacuum-assisted filtration;(b) SEM image of the MXene/SnS2-5∶1;(c, d) HRTEM images of CoS/MXene;(e) The synthesis process of CoS/MXene composite;(f) Cycling performance of MXene/SnS2 10∶1, MXene/SnS2 5∶1, MXene/SnS2 2∶1 and MXene;(g) Rate performance of CoS/MXene at various current densities[43, 44].Copyright 2018, Elsevier; Copyright 2019, Elsevier
图6 (a, b)CoNiO2/Ti3C2Tx的透射电子显微镜图像;(c)CoNiO2/Ti3C2Tx的循环性能;(d)CoNiO2/Ti3C2Tx的电荷转移机制[63]
Fig. 6 (a, b) TEM images of CoNiO2/Ti3C2Tx;(c) Cycling performance of CoNiO2/Ti3C2Tx composite;(d) Charge-transfer mechanism of CoNiO2/Ti3C2Tx composite[63]. Copyright 2018, Elsevier
图7 (a)制备钛酸钠或钛酸钾纳米带的示意图;(b, c)钛酸钾的扫描电子显微镜图像(b: 插图是钛酸钾粉末);(d)钛酸钾的高分辨透射电子显微镜图像(插图是相应的SAED);(e)在0.1 mV·s-1 钛酸钾的循环伏安曲线;(f)钛酸钾在各种电流密度下(20~300 mA·g-1)的充放电曲线[80]
Fig. 7 (a) Schematic of the fabrication of M-NTO or M-KTO nanoribbons;(b, c) SEM images of M-KTO(The inset is the photograph of M-KTO powder);(d) HRTEM image of M-KTO(The inset is the corresponding SAED patterns);(e) CV of M-KTO measured at 0.1 mV·s-1;(f) Galvanostatic charge and discharge curves of M-KTO cycled at different current densities[80]. Copyright 2017, American Chemical Society
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doi: 10.1021/acsnano.7b01165     URL     pmid: 28460161
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