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化学进展 2024, Vol. 36 Issue (3): 319-334 DOI: 10.7536/PC230716 前一篇   后一篇

• 综述 •

二维层状沸石的合成及其催化、吸附与分离应用

胡诗雨1, 闫玥儿2,*(), 张亚红1, 王振东3, 唐颐1,*()   

  1. 1 复旦大学 化学系 上海 200438
    2 复旦大学 中华古籍保护研究院 上海 200433
    3 中石化（上海）石油化工研究院有限公司 绿色化工与工业催化全国重点实验室 上海 201208
  • 收稿日期:2023-07-18 修回日期:2023-11-21 出版日期:2024-03-24 发布日期:2024-02-26
  • 基金资助:
    国家重点研发计划(2018YFA0209402); 国家自然科学基金(22072028); 国家自然科学基金(22088101); 上海市自然科学基金(22ZR1407200)
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Synthesis of Two-Dimensional Layered Zeolites and Their Catalysis, Adsorption and Separation Applications

Shiyu Hu1, Yueer Yan2(), Yahong Zhang1, Zhendong Wang3, Yi Tang1()   

  1. 1 Department of Chemistry, Fudan University, Shanghai 200438, China
    2 Institute for Preservation and Conservation of Chinese Ancient Books, Fudan University, Shanghai 200433, China
    3 State Key Laboratory of Green Chemical Engineering and Industrial Catalysis, SINOPEC Shanghai Research Institute of Petrochemical Technology Co., Ltd., Shanghai 201208
  • Received:2023-07-18 Revised:2023-11-21 Online:2024-03-24 Published:2024-02-26
  • Contact: * e-mail: yueeryan@fudan.edu.cn (Yueer Yan); yitang@fudan.edu.cn (Yi Tang)
  • Supported by:
    National Key R&D Program of China(2018YFA0209402); National Natural Science Foundation of China(22072028); National Natural Science Foundation of China(22088101); Shanghai Natural Science Foundation(22ZR1407200)

与三维沸石相比，二维层状沸石具有更大的表面积、更短的扩散距离和更具韧性的结构，在许多领域中都具有更大优势。近年来，二维层状沸石的研究已成为新热点。本文基于前期文献调研总结，从两类合成角度（Bottom-up和Top-down法）归纳了近年来二维沸石的合成方法，重点综述了同种类型沸石的不同合成法的进展。此外，本文简述了二维沸石在催化、吸附和分离领域中的应用，并展望了二维沸石广阔的应用前景，以期为二维沸石的合成与应用提供参考。

关键词： 二维沸石, 合成, 酸催化, 吸附, 分离膜

Compared with three-dimensional zeolites, two-dimensional layered zeolites have greater advantages in many fields, with larger surface area, shorter diffusion distance and more ductile structure. In recent years, the research on two-dimensional layered zeolites has become a new hotspot. Based on previous research and summary, this article summarizes the synthesis methods of two-dimensional zeolites in the past five years from two types of synthesis perspectives (bottom-up and top-down methods), with a focus on reviewing the progress of different synthesis methods for the same topology of zeolite. In addition, this article briefly describes the applications of two-dimensional zeolites in the fields of catalysis, adsorption, and separation and looks forward to the broad application prospects of two-dimensional zeolites so as to provide theoretical guidance and reference basis for the synthesis and application of two-dimensional zeolites.

Contents

1 Introduction

2 Synthesis of two-dimensional layered zeolites

2.1 Bottom-up synthesis method

2.2 Top-down synthesis method

3 Application of two-dimensional layered zeolite

3.1 Catalysis

3.2 Adsorption

3.3 Separation membrane

4 Conclusion and outlook

Key words: 2D zeolite, synthesis, acid catalysis, adsorption, separation membrane
()
图1 IZA已认定的沸石拓扑结构，黄色图标为已确认的具有层状形式的结构
Fig. 1 Zeolite frameworks approved by the IZA Structure Commission in the alphabetical order and the confirmed structures with layered forms (yellow)
图2 二维沸石自下而上合成示意图
Fig. 2 Schematic diagram of bottom-up synthesis of 2D zeolite
图3 一步法制备表面增强活性二维MWW型沸石纳米晶层[38]
Fig. 3 Enhanced surface activity of MWW zeolite nanosheets prepared via a one-step synthesis[38]. Copyright ? 2020, American Chemical Society
图4 用C22-6-6/TPAOH摩尔比为10/0（a）、10/1（b）、10/2（c）、10/3（d）、10/5（e）、10/8（f）、10/12（g）和10/20（h）制备的MFI沸石的扫描电子显微镜（SEM）图像[44]。Si/Al比为~40（i）的商用MFI沸石作为对照
Fig. 4 SEM images of MFI zeolites obtained with C22-6-6/TPAOH molar ratio of (a) 10/0, (b) 10/1, (c) 10/2, (d) 10/3, (e) 10/5, (f) 10/8, (g) 10/12, and (h) 10/20, respectively, in the dual template synthesis. (i) Commercial MFI with Si/Al ratio of ～40 was used for comparison[44]. Copyright ? 2014, American Chemical Society
图5 二维沸石自上而下合成示意图
Fig. 5 Schematic diagram of top-down synthesis of 2D zeolite
图6 不同硅锗比水解沸石的SEM图像[62]。ITH-4（A）, ITH-10（B）, ITR-2（C）, ITR-3（D）, 0.1B-IWR-2（E）, 0.1B-IWR-6（F）, and 0.1B-IWR-2（G）
Fig. 6 SEM image of ITH-4 (A), ITH-10 (B), ITR-2 (C), ITR-3 (D), 0.1B-IWR-2 (E), 0.1B-IWR-6 (F), and 0.1B-IWR-2 (G)[62]. Copyright ? 2014, American Chemical Society
图7 三步离散操作（a）和一次性操作（b）条件下二维沸石气相柱撑（VPP）实验示意图[25]
Fig. 7 Schematic diagram of two-dimensional zeolite vapor phase column (VPP) experiment under three-step discrete operation (a) or one-time operation conditions (b)[25] Copyright ? 2019, American Chemical Society
图8 MCM-22(P)柱撑工艺[72]
Fig. 8 Illustration showing the reversible swelling of MCM-22(P) and pillaring of the swollen material[72]. Copyright ? 2008, American Chemical Society
图9 （a）纯MFI微粒与（b~e）BMLM粒子在不同水浓度合成条件下的SEM图像[102]
Fig. 9 SEM images of (a) 10 μm bare MFI and (b~e) BMLM particles at varying water concentrations in the synthesis [102]. Copyright ? 2012, American Chemical Society
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