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化学进展 2024, Vol. 36 Issue (1): 67-80 DOI: 10.7536/PC230516 前一篇   后一篇

• 综述 •

四苯乙烯基共价有机框架的设计、合成及应用

王子情1, 杜金峰2, 陆福泰1,2,*(), 邓启良1,2,*   

  1. 1 天津科技大学理学院 天津 300457
    2 天津科技大学化工与材料学院 天津 300457
  • 收稿日期:2023-05-17 修回日期:2023-07-28 出版日期:2024-01-24 发布日期:2023-08-06
  • 作者简介:

    陆福泰 天津科技大学化工与材料学院硕士生导师，2012年于天津大学获得博士学位，主要从事金属有机框架材料和共价有机框架材料研究，主持国家自然科学基金1项,发表SCI论文10余篇。

    邓启良 天津科技大学化工与材料学院教授，博士生导师，天津市色谱学会副秘书长，首批天津市中青年科技创新领军人才，Current Chinese Science编委，国家自然科学基金评审专家，教育部博士、硕士论文评审专家，《分析化学》、《色谱》、Biosensors and Bioelectronics、Chemical communication、Sensors and Actuators B Chemical等国内外著名期刊审稿专家。发表SCI论文90篇，他引1200余次，申请国家发明专利17件，其中11件获得授权。先后主持国家自然科学基金三项、科技部“科技支撑计划”项目三项，编写中、英文专著各一部。

  • 基金资助:
    国家自然科学基金(2190080961)
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Tetraphenylethene-Based Covalent Organic Frameworks (COFs): Design, Synthesis and Applications

Ziqing Wang1, Jinfeng Du2, Futai Lu1,2(), Qiliang Deng1,2   

  1. 1 College of Sciences, Tianjin University of Science and Technology, Tianjin 300457, China
    2 College of Chemical Engineering and Materials Science, Tianjin University of Science and Technology, Tianjin 300457, China
  • Received:2023-05-17 Revised:2023-07-28 Online:2024-01-24 Published:2023-08-06
  • Contact: * e-mail: lufutai@tust.edu.cn
  • Supported by:
    National Natural Science Foundation of China(2190080961)

共价有机框架（COFs）作为一类新型的结晶多孔材料，是由构筑单元通过共价键自组装而成。COFs具有孔道规整、热稳定性高、结晶度高、结构可调等特点，因此在气体存储与分离、催化、质子传导、储能材料、光电、传感以及生物医学等领域具有广泛的应用。近年来，四苯乙烯基共价有机框架（TPE-based COFs）因其聚集诱导发光效应明显、合成简单、易功能化而备受关注。本文简述了四苯乙烯基COFs的构筑单元、拓扑结构、合成策略，以及其在不同领域的应用进展。最后指出了四苯乙烯基COFs的发展前景以及可能面临的挑战。

关键词： 四苯乙烯, 共价有机框架, 构筑单元, 拓扑, 应用

Covalent organic frameworks (COFs) as a new class of crystalline porous materials are assembled by appropriate building blocks through covalent bonds. COFs have been utilized in many fields such as storage and separation of gases, catalysis, proton conduction, energy storage, optoelectronics, sensing and biomedicine due to their regular channels, high thermal stability, high crystallinity and adjustable structure. In recent years, tetraphenylethylene-based covalent organic frameworks (TPE-based COFs) have attracted much attention due to their obvious aggregation induced luminescence effect, simple synthesis and easy functionalization. In this paper, the construction units, topological structures, synthesis strategies and application progress of TPE-based COFs in different fields are briefly reviewed. Finally, the development prospects and possible challenges of TPE-based COFs are pointed out.

Contents

1 Introduction

2 Construction unit and topological structure of TPE-based COFs

3 Synthesis strategy of TPE-based COFs

4 Applications

4.1 Catalysis

4.2 Adsorption

4.2.1 Ions adsorption

4.2.2 Gas adsorption

4.2.3 Biomolecule adsorption

4.3 Sensors

4.3.1 Sensors for detecting explosives

4.3.2 Ion sensors

4.3.3 Acid-base sensors

4.3.4 Enantioselective sensors

4.3.5 Biosensors

4.4 Optoelectronic

4.4.1 Light emitting diode

4.4.2 Electrochemical energy storage

4.4.3 Others

4.5 Bio-related applications

5 Prospects and challenges

Key words: tetraphenylethylene, covalent organic frameworks, building blocks, topology, applications
()
图1 用于合成四苯乙烯基COFs的单体
Fig. 1 Monomers for use in the synthesis of TPE-based COFs
图2 成功用于合成四苯乙烯基COFs的构筑单元
Fig. 2 Building units successfully used for the synthesis of TPE-based COFs
图3 用于四苯乙烯基COFs的键连方式
Fig. 3 Linkages used in TPE-based COFs
图4 四苯乙烯基COFs的拓扑结构
Fig. 4 Topological structures of TPE-based COFs
图5 TP-COF的合成路线及可见光下光催化析氢过程[55]
Fig. 5 The synthetic route of TP-COF and the process of photocatalytic H2 evolution under visible light[55]
图6 （a）273 K时NAT-COF C3H8, C2H6, C2H4和CH4的气体吸附[65]；（b）SCU-COF-2粉末填充柱穿透实验示意图[69]
Fig. 6 (a) Gas adsorption of C3H8, C2H6, C2H4 and CH4 for NAT-COF at 273 K[65]; (b) The schematic diagram of breakthrough experiments in the columns packed with SCU-COF-2 powder[69]
图7 丙酮中加入TNP （0~25 ppm）后Py-TPE-COF的荧光猝灭实验[72]
Fig. 7 Fluorescence quenching experiments of the Py-TPE-COF upon addition of TNP (0-25 ppm) in acetone[72]
图8 （a） COF-DHTA的Al3+传感过程[75]；（b） TTPE-COF在293 K下对水、苯和甲苯的吸附等温线，以及在365 nm紫外灯下的荧光照片[67]
Fig. 8 (a) Al3+ sensing mechanism of COF-DHTA[75]; (b) Water, benzene, and toluene adsorption isotherms of the TTPE-COF at 293 K, and the fluorescence photographs under a 365 nm UV lamp[67]
图9 TFA熏蒸不同时间后试纸的荧光发射光谱以及TFA蒸气和TEA蒸气（λex = 365 nm）作用下试纸的光学照片[78]
Fig. 9 Fluorescence emission spectra of test paper fumigated by TFA at different times and optical photographs of test paper upon exposure to TFA vapour and TEA vapour (λex= 365 nm)[78]
图10 7@PVDF暴露于α-蒎烯后的下降百分比[80]
Fig. 10 Decrease percentage upon exposure to α-pinene for 7@PVDF[80]
图11 用L-苯丙氨酸滴定NUS-30纳米片的Stern-Volmer图和NUS-30纳米片的AFM图像[82]
Fig. 11 Stern-Volmer plots of NUS-30 nanosheets being titrated with L-phenylalanine and AFM images of NUS-30 nanosheets[82]
图12 （a）PT-COF的电容储存过程[40]；（b）钙钛矿电池的能级图和示意图[39]
Fig. 12 (a) The capacitor storage process of PT-COF[40]; (b) The energy-level diagram and schematic illustration of the PVSCs[39]
图13 COFTFBE?PDAN@FeIIITA-PEI的制备和用于目标肿瘤细胞的发光成像和铁死亡的示意图[86]
Fig. 13 Schematic illustration of the preparation of COFTFBE?PDAN@FeIIITA-PEI for luminescence imaging and ferroptosis in target tumor cells[86]
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