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化学进展 2021, Vol. 33 Issue (12): 2404-2412 DOI: 10.7536/PC210103 前一篇   

• 综述 •

碘氧化铋光催化剂的合成、改性及净化一氧化氮

周汉强1, 于明飞1, 陈巧珊1,*(), 王建春2,*(), 毕进红1,*()   

  1. 1 福州大学环境与资源学院 福州 350108
    2 福建龙净环保股份有限公司 厦门 361000
  • 收稿日期:2021-01-08 修回日期:2021-03-12 出版日期:2021-12-20 发布日期:2021-07-29
  • 通讯作者: 陈巧珊, 王建春, 毕进红
  • 基金资助:
    国家自然科学基金项目(5167204); 福建省自然科学基金面上项目(2019J01648)
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Synthesis, Modification of Bismuth Oxyiodide Photocatalyst for Purification of Nitric Oxide

Hanqiang Zhou1, Mingfei Yu1, Qiaoshan Chen1(), Jianchun Wang2(), Jinhong Bi1()   

  1. 1 College of Environment and Resources, Fuzhou University,Fuzhou 350108, China
    2 Fujian Longking Co. Ltd,Xiamen 361000, China
  • Received:2021-01-08 Revised:2021-03-12 Online:2021-12-20 Published:2021-07-29
  • Contact: Qiaoshan Chen, Jianchun Wang, Jinhong Bi
  • Supported by:
    the National Natural Science Foundation of China(5167204); the Natural Science Foundation of Fujian Province(2019J01648)

光催化技术因其节能、高效、无二次污染等特点,在低浓度一氧化氮(NO)污染治理方面展现出了巨大潜力。在众多半导体材料中,碘氧化铋(BiOI)光催化剂具有窄带隙和独特的层状结构,有利于可见光吸收和电子空穴对分离,展现出了良好的光催化活性和稳定性,近十几年来备受关注。本文综述了BiOI半导体材料光催化净化NO的最新研究进展,阐述了BiOI晶体形貌与晶面调控对其光催化性能的影响;重点介绍了各类改性方法如表面修饰、离子掺杂、异质结构筑等对BiOI光催化活性的提升机制,并提出了该研究方向所面临的挑战与应用前景,旨在为设计高活性BiOI基光催化材料以及高效处理低浓度NO污染提供理论借鉴与技术支撑。

关键词： 碘氧化铋, 一氧化氮, 光催化, 大气污染

Photocatalytic technology has shown great potential for purification of low-concentration nitric oxide (NO) pollution due to its energy-saving property, high efficiency, and limited secondary pollution. Among various semiconductors, bismuth oxyiodide (BiOI) photocatalyst has drawn considerable attention in recent years due to the superior photocatalytic activity and stability, since its narrow band gap and specific layered structure is in favor of visible light absorption and electron-hole pairs separation. Hence, we overview the latest research progress in the photocatalytic purification of NO by BiOI and introduce the influence of crystalline morphology and facets on its photocatalytic performance. The modification and activity enhancement mechanism of BiOI is emphatically expounded, for example, surface modification, ion doping and heterostructure construction. The future prospects and challenges in this research spot are put forward for the sake of providing theoretical reference and technical support for the design of highly active BiOI and the efficient purification of low concentration NO.

Contents

1 Introduction

2 Reaction mechanism and pathway of photocatalytic purification of NO

3 Controlled synthesis of bismuth oxyiodide

3.1 Morphological control

3.2 Crystal plane control

4 Surface modification and ion doping of bismuth oxyiodide

5 Construction of bismuth oxyiodide heterojunction

5.1 Bismuth oxyiodide/semiconductor heterojunction

5.2 Bismuth oxyiodide/insulator heterojunction

5.3 Ternary heterojunction

6 Conclusion and outlook

Key words: bismuth oxyiodide, nitric oxide, photocatalysis, atmospheric contamination
()
图1 近十年来每年发表的关于光催化净化NO的文章数量(资料来源:Web of Science)
Fig.1 Numbers of annually published articles on photocatalytic NO purification in recent ten years (Source: Web of Science)
图2 (a)BiOI的晶体结构及其(b)可见光催化净化NO的机理图
Fig.2 (a)Crystal structure of BiOI and (b) the schematic illustration of photocatalytic purification of NO based upon BiOI under visible light
图3 (a~c)球状和(d~f)片状 BiOI的扫描电镜(SEM)图[37]
Fig.3 (a~c)SEM images of as-synthesized BiOI spheres and (d~f) plates[37]. Copyright 2019, IOP Publishing Ltd
表1 表面修饰及离子掺杂改性BiOI净化NO的效率
Table 1 Removal efficiency of NO by surface modification and ion-doped modification of BiOI
Catalyst Modified element Dosage Light source Concentration and time Photocatalytic activity ref
BiOI Bi 0.1 g 150 W halogen tungsten lamp,λ > 420 nm 600 ppb, 30 min 40.8% 47
BiOI Bi 0.2 g 150 W lamp, λ > 420 nm ppb levels, 30 min 51.4% 48
BiOI Bi 0.05 g 500 W Xe lamp 500 ppb, 1 h 46.5% 49
Bi5O7I Er 0.1 g 300 W Xe lamp 450 ppb, 30 min 54.0% 50
BiOI Zn 0.1 g 300 W Xe lamp, λ > 420 nm 430 ppb, 30 min 53.6% 42
Bi5O7I La
Au
La、Au		 / 300 W Xe lamp, λ > 420 nm 400 ppb, 30 min 42.7%
34.2%
52.5%		 51
图4 3%Zn-BiOI 在黑暗和可见光照射下光氧化去除NO的机理[42]
Fig.4 Schematic illustration of the photo-oxidative removal of NO by 3%Zn-BiOI in the dark and under visible light irradiation[42]. Copyright 2019, American Chemical Society
图5 Bi2WO6/BiOI垂直异质结构表面NO的光氧化机理示意图[54]
Fig.5 Schematic representation of NO photooxidation mechanism on the surface of Bi2WO6/BiOI vertical heterostructure[54]. Copyright 2019, Wiley
表2 BiOI异质结净化NO的效率
Table 2 Removal efficiency for NO by BiOI heterojunction
Catalyst Dosage Light source Concentration and time Photocatalytic activity Ref
BiOI/BiOCl 0.15 g 300 W halogen tungsten lamp, λ > 400 nm 450 ppb, 30 min 54.6% 53
BiOBr/BiOI 0.15 g Xe lamp, λ > 420 nm 600 ppb, 50 min 57% 28
Bi2WO6/BiOI 0.2 g 150 W Xe lamp, λ > 420 nm 500 ppb, 30 min 40% 54
Bi2O2CO3/BiOI 0.2 g 150 W halogen tungsten lamp, λ > 420 nm 600 ppb, 30 min 50.8% 55
BiOIO3/BiOI 0.1 g 150 W halogen tungsten lamp, λ > 420 nm 550 ppb, 30 min 41.3% 56
BiOI/La(OH)3 0.1 g 150 W halogen tungsten lamp, λ > 420 nm 520 ppb, 30 min 50.5% 57
SrTiO3/BiOI 0.2 g λ > 420 nm ppb levels, 30 min 59% 58
BiOI/ZnWO4 0.1 g 300 W Xe lamp, λ > 420 nm 430 ppb, 30 min 48.24% 59
SrCO3/BiOI 0.2 g λ > 420 nm ppb levels, 30 min 48.3% 27
BaCO3/BiOI 0.2 g λ > 420 nm ppb levels, 30 min 47.5% 60
CaSO4/BiOI 0.2 g λ > 420 nm ppb levels, 30 min 54.4% 61
BiOBr0.5I0.5/BiOBr/BiOI 0.15 g Xe lamp, λ > 420 nm 750 ppb, 15 min 48% 62
Bi/BiOI/Bi2O2CO3 0.2 g 150 W halogen tungsten lamp, λ > 420 nm 550 ppb, 30 min 50.7% 63
Bi/BiOI/graphene 0.1 g 300 W Xe lamp, λ > 420 nm 430 ppb, 30 min 51.8% 64
图6 (a)BiOI(001)面和BiOIO3(010)面侧视图以及(b)BiOI在BiOIO3 (010)面上的生长示意图[56]
Fig.6 The side view of the (001) plane of BiOI and the (010) plane of BiOIO3 (a) and the schematic diagram of BiOI grown on the (010) facets of BiOIO3 (b)[56]. Copyright 2015, Royal Society of Chemistry
图7 绝缘体-半导体异质结上光生载流子的分离和转移及光催化过程示意图[60]
Fig.7 Schematic diagram for the separation and transfer of photogenerated carriers and the photocatalytic process over the insulator-semiconductor heterojunction[60]. Copyright 2018, Royal Society of Chemistry
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