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化学进展 2020, Vol. 32 Issue (9): 1334-1343 DOI: 10.7536/PC200101 前一篇   后一篇

• 综述 •

搅拌棒吸附萃取技术

刘育坚1, 刘智敏1, 许志刚1,**(), 李攻科2,**()   

  1. 1. 昆明理工大学理学院 昆明 650500
    2. 中山大学化学学院 广州 510275
  • 收稿日期:2020-01-02 修回日期:2020-02-24 出版日期:2020-09-24 发布日期:2020-06-30
  • 通讯作者: 许志刚, 李攻科
  • 作者简介:
    **Corresponding author e-mail: (Zhigang Xu); (Gongke Li)
  • 基金资助:
    *国家自然科学基金项目(21565018)
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Stir Bar Sorptive Extraction Technology

Yujian Liu1, Zhimin Liu1, Zhigang Xu1,**(), Gongke Li2,**()   

  1. 1. Faculty of Science, Kunming University of Science and Technology, Kunming 650500, China
    2. School of Chemistry, Sun Yat-Sen University, Guangzhou 510275, China
  • Received:2020-01-02 Revised:2020-02-24 Online:2020-09-24 Published:2020-06-30
  • Contact: Zhigang Xu, Gongke Li
  • Supported by:
    the National Natural Science Foundation of China(21565018)

搅拌棒吸附萃取技术的提出至今已有二十年,其源于固相微萃取,却有更高的固定相体积、萃取容量和萃取回收率。搅拌棒吸附萃取作为一种高效的样品前处理方法,广泛应用于环境样品、食品样品、药物样品和挥发性物质的分离富集。搅拌棒的核心是涂层,目前已有商品化涂层、自制分子印迹聚合物涂层和自制非印迹涂层。本文介绍了搅拌棒吸附萃取的基本原理,系统评述了各种搅拌棒吸附萃取涂层的发展和应用研究进展,并介绍了一些新颖的搅拌棒萃取模式,最后对搅拌棒吸附萃取技术的发展进行了总结和展望。

关键词： 搅拌棒吸附萃取, 涂层, 样品前处理, 分子印迹聚合物

Stir bar sorptive extraction(SBSE) has been proposed about 20 years. It originates from solid phase microextraction, but has higher stationary phase volume, extraction capacity and extraction recovery. Stir bar sorptive extraction, as an efficient sample pretreatment method, is widely used for analytes enrichment in environmental samples, food samples, pharmaceutical samples and volatile substances. The core of the stir bar is the coating. Currently, there are commercial coatings, molecularly imprinted polymer coatings, and non-imprinted coatings. This paper introduces the basic principles of stir bar sorptive extraction. The development and application of various stir bar sorptive extraction coatings are systematically reviewed. Some novel stir bar sorptive extraction modes are also briefly introduced in this review. Finally, the development of stir bar sorptive extraction technology is summarized and prospected.

Contents

1 Introduction

2 Development and application of SBSE coatings

2.1 Commercial coatings of stir bar

2.2 Polymeric coatings of stir bar

2.3 Molecularly imprinted polymer stir bar coatings

2.4 Other coatings and SBSE modes

3 Conclusion and outlook

Key words: stir bar sorptive extraction, coatings, sample pretreatment, molecularly imprinted polymers
()
图1 1999年以来SBSE发表的文献数量(数据库:Web of Science,检索词:stir bar sorptive extraction,检索时间:2019-12-20)
Fig.1 Publications about SBSE since 1999(Source: Web of Science, Keyword: stir bar sorptive extraction, Search time: 2019-12-20)
图2 SPME和SBSE的理论回收率比较[7]
Fig.2 Theoretical recovery(%) as function of solute logK O/W for SPME and SBSE [7]
图3 双搅拌棒吸附萃取的示意图[35]
Fig.3 Dual stir bar sorptive extraction methodology[35]
图4 多搅拌棒吸附萃取示意图[37]
Fig.4 Images of multi-SBSE set-up [37]
图5 连续搅拌棒吸附萃取示意图[38]
Fig.5 Experimental set-up of sequential SBSE [38]
表1 溶胶-凝胶法制备改性PDMS搅拌棒涂层
Table 1 Preparation of modified PDMS stir bar coating by sol-gel method
Analytes Coating Detection Samples ref
environment sample oestrogen PDMS/β-CD HPLC water and leachate of disposable tableware 46
brominated flame retardant compounds PDMS/β-CD,PEG/PDMS/PVA HPLC soil and dust 47
hydrocarbonspolycyclic aromatic PDMS/β-CD/divinylbenzene HPLC lake water and soil 48
steroid hormone PDMS/β-CD/trimethylphenylsilane APCI-MS/MS water 49
phenol amino multi-walled carbon nanotubes/PDMS HPLC environmental water and soil 50
organophosphorus pesticide PDMS/polythiothene GC environmental water 51
oestrogen PDMS/MOF-5 HPLC environmental water 52
PDMS/MOF-199
hydrocarbonspolycyclic aromatic PDMS/IRMOF-3
PDMS/Al-MIL-53-NH2 HPLC environmental water 53
triazine carboxyl multiwalled carbon nanotubes/PDMS PGD-IMS environmental water and soil 54
phenol PDMS/covalent triazine framework HPLC environmental water 55
organophosphorus pesticide PDMS/MIL-101-Cr-NH2 GC environmental water 56
triazine MIL-100(Fe)/PDMS HPLC environmental water 57
MIL-101(Cr)/PDMS
UiO-66/PDMS
pyran PDMS/triethoxysilyl nitrile HPLC environmental water 58
4, 4'-bipyridine monohydroxy cucurbit[7]/PDMS HPLC water 59
food sample organophosphorus pesticide PDMS/PVA GC honey 60
organophosphorus pesticide TEOS/PDMS HPLC water 61
pesticide PDMS/activated carbon GC-MS sugar cane juice 62
oestrogen PDMS/β-CD/divinylbenzene HPLC pork and chicken 63
preservative PDMS/C18 HPLC beverage 64
microcystin HLB/PDMS HPLC shellfish 65
pharmaceutical sample antidepressant PDMS/polypyrrole HPLC blood plasma 66
ketoprofen and diclofenac PDMS/triethoxysilyl nitrile CE water 67
thyroid hormone PEG/PDMS/γ- mercaptopropyltrimethoxysilane HPLC/ICP-MS urea 68
other volatile organic sulfur compounds PEG/PDMS/PVA GC water 69
volatile organic selenium compounds PEG/PDMS/PVA GC-ICP-MS garlic and onion 70
图6 单羟基瓜环[7]/PDMS与其他涂层的萃取效率比较[59]
Fig.6 Comparison of extraction efficiencies between monohydroxycucurbit[7]uril/PDMS and other coatings[59]
图7 单壁碳纳米角多孔甲基丙烯酸酯整体材料示意图[86]
Fig.7 Porous methacrylate monoliths with oxidized single-walled carbon nanohorns[86]
图8 将MIL-68共价固定在PEEK管上的搅拌棒吸附萃取[95]
Fig.8 Covalent immobilization of MIL-68 onto PEEK jacket for stir bar extraction[95]
图9 “杠铃形”搅拌棒实物图[110]
Fig.9 Photo of barbell-shaped stir bar[110]
图10 新的搅拌棒吸附萃取技术。(A)搅拌杆吸附萃取[125];(B)旋转盘吸附萃取[126];(C)搅拌饼吸附萃取[127]
Fig.10 Novel extraction techniques for SBSE.(A) Stir rod sorptive extraction [125];(B) Rotating disk sorptive extraction [126];(C) Stir cake sorptive extraction[127]
图11 MISBSE-HPLC系统示意图[130]
Fig.11 Schematic representation of MISBSE-HPLC system [130]
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