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化学进展 2017, Vol. 29 Issue (11): 1366-1394 DOI: 10.7536/PC170559 前一篇   后一篇

• 综述 •

四氧化三铁纳米材料的制备与应用

朱脉勇*, 陈齐, 童文杰, 阚加瑞, 盛维琛   

  1. 江苏大学材料科学与工程学院 镇江 212013
  • 收稿日期:2017-05-27 修回日期:2017-10-10 出版日期:2017-11-15 发布日期:2017-10-27
  • 通讯作者: 朱脉勇,e-mail:maiyongzhu@ujs.edu.cn E-mail:maiyongzhu@ujs.edu.cn
  • 基金资助:
    国家自然科学基金项目（No.21403091），江苏省自然科学基金项目（No.BK20130486）和江苏大学优秀人才启动基金（No.12JDG093）资助
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Preparation and Application of Fe3O4 Nanomaterials

Maiyong Zhu*, Qi Chen, Wenjie Tong, Jiarui Kan, Weichen Sheng   

  1. School of Materials Science & Engineering, Jiangsu University, Zhenjiang 212013, China
  • Received:2017-05-27 Revised:2017-10-10 Online:2017-11-15 Published:2017-10-27
  • Supported by:
    The work was supported by the National Natural Science Foundation of China (No. 21403091), the Natural Science Foundation of Jiangsu Province (No. BK20130486), and the Project Funded by Jiangsu University for Senior Intellectuals (No. 12JDG093).
近年来磁性Fe3O4纳米材料因其独特的物理化学性质如量子尺寸效应、表面界面效应、电学特性以及磁学特性等，而引起了广泛的研究，并在诸多领域（如环境、能源）具有潜在应用前景。本文总结了近年来国内外制备Fe3O4的一些方法，主要包括：沉淀法、热分解法、水热法、微乳液法以及溶胶-凝胶法，同时对各种制备方法的优缺点进行了比较。在应用方面，着眼于Fe3O4良好的磁响应性，综述了Fe3O4纳米材料及其复合物作为吸附剂用于去除废水中的金属离子以及有机污染物；系统总结了Fe3O4在催化中的应用，包括其本身作为催化剂和作为催化剂活性组分（如贵金属纳米粒子、金属氧化物半导体纳米光催化剂、金属有机化合物等）的载体两个方面。另外，本文还介绍了Fe3O4纳米材料在能源存储（锂离子电池和超级电容器）以及生物医药（肿瘤诊疗、固定化酶和免疫分析）等方面的应用。最后，针对目前Fe3O4纳米材料在制备中存在的一些问题进行探讨并对今后的研究方向进行了展望。
关键词： Fe3O4, 环境处理, 化学催化, 能源存储, 生物医药
Magnetic Fe3O4 nanomaterials, possessing unique physicochemical properties such as quantum size effect, surface interfacial effect, electrical properties and magnetic properties, have attracted intensive research interest and shown potential applications in many fields (such as enviroment, energy) during the past years. In this review, some methods for preparing Fe3O4 in recent years are summarized, including precipitation method, thermal decomposition method, hydrothermal method, microemulsion method and sol-gel method. The advantages and disadvantages of various preparation methods are compared. As for the application of Fe3O4 nanomaterials, the article firstly summarizes their application as adsorbent for removal of heavy metal ions and organic pollutants from wastewater. The application of Fe3O4 nanomaterials in catalysis, including Fe3O4 nanomaterials acting active species and acting as supports for active species (such as noble metal nanoparticles, transition metal oxide, as well as metallic organic compounds) is also overviewed in detail. While applied in environment treatment and chemical catalysis, the largest advantage of Fe3O4 nanomaterials is that they can be easily separated by magnetic separation. Furthermore the application of Fe3O4 nanomaterials in energy storage (such as lithium-ion batteries and super capacitors) and biomedicine (tumor diagnosis and treatment, immobilized enzyme and immunoassay) are also discussed in brief. Finally, some problems in the preparation of Fe3O4 nanomaterials and their future research directions are outlined.
Contents
1 Introduction
2 Synthesis strategies of Fe3O4 nanomaterials
2.1 Precipitation method
2.2 Hydrothermal method
2.3 Thermal decomposition
2.4 Sol-gel method
2.5 Microemulsion method
2.6 Other methods
3 Applications of Fe3O4 nanomaterials
3.1 Environmental treatment
3.2 Chemical catalysis
3.3 Energy storage
3.4 Biomedical
3.5 Other applications
4 Conclusion
Key words: Fe3O4, environmental treatment, chemical catalysis, energy storage, biomedicine

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