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化学进展 2017, Vol. 29 Issue (9): 1127-1141 DOI: 10.7536/PC170610 前一篇   后一篇

• 综述 •

基于新型材料的固相微萃取探针的制备与应用

殷立, 徐剑桥*, 黄周兵, 陈国胜, 郑娟, 欧阳钢锋*   

  1. 中山大学化学学院 环境与能源化学广东普通高校重点实验室 广州 510275
  • 收稿日期:2017-06-06 修回日期:2017-08-30 出版日期:2017-09-15 发布日期:2017-09-05
  • 通讯作者: 欧阳钢锋,e-mail:cesoygf@mail.sysu.edu.cn;徐剑桥,e-mail:522688270@qq.com E-mail:cesoygf@mail.sysu.edu.cn;522688270@qq.com
  • 基金资助:
    国家自然科学基金项目（No.21377172，21477166，21527813，21677182）资助
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Solid-Phase Microextraction Fibers Based on Novel Materials:Preparation and Application

Li Yin, Jianqiao Xu*, Zhoubing Huang, Guosheng Chen, Juan Zheng, Gangfeng Ouyang*   

  1. Key Laboratory of Environment and Energy Chemistry of Guangdong Higher Education Institutes, School of Chemistry, Sun Yat-sen University, Guangzhou 510275, China
  • Received:2017-06-06 Revised:2017-08-30 Online:2017-09-15 Published:2017-09-05
  • Supported by:
    The work was supported by the National Natural Science Foundation of China (No. 21377172, 21477166, 21527813, 21677182).
固相微萃取（SPME）是一种简便、快速、绿色的样品前处理方法，近年来引发了广泛关注。固相微萃取探针的萃取相对其萃取选择性和效率起着决定性作用，因此一系列物理化学性质优秀的新型固相微萃取涂层材料应运而生，被用于制备新型固相微萃取探针，以对不同样品基质中的有机小分子进行检测。本文概述了近年来新型SPME探针的研制所依托的新型材料，包括聚合物材料、碳材料、金属有机框架材料等，并重点阐述了相关材料的制备与固定方法、微观结构与萃取性能，以及所制备探针在环境分析、纺织品和皮革分析、食品分析等领域中的应用，并进一步对新型固相微萃取涂层今后的开发方向和应用前景进行了展望。
关键词： 固相微萃取, 新材料, 探针, 有机污染物, 环境分析
Convenient, rapid as well as environmentally-friendly, solid-phase microextraction is(SPME) a sample preparation technique, which draws widespread attention among the scientific community. The extraction phases in the SPME fibers determine their selectivity and extraction efficiency, hence, a series of new fiber coatings with excellent physical and chemical properties are developed for detection of various small organic molecules in complex sample matrices. Herein, we give a brief review of some materials widely used for the preparation of new SPME fibers, including polymers, carbonaceous materials, metal-organic framework, and some other materials, with the emphasis on the fiber preparation methodologies, the microstructures and extraction properties of the novel fiber coatings, together with applications of the synthesized fibers on environmental analysis, food analysis and inspection on textile and leather samples. Furthermore, future developing trends and application prospects of the new fiber coatings are discussed.
Contents
1 Introduction
2 Polymers
2.1 Commonly used polymers
2.2 Porous polymers
2.3 Molecularly-imprinted polymers
2.4 Polyelectrolytes
2.5 Electrospining
3 Carbonaceous materials
3.1 Graphene
3.2 Carbon nanotubes
3.3 Porous carbons
4 Metal-organic framework
4.1 MIL
4.2 MAF
4.3 Bio-MOFs
4.4 MOF@IL
4.5 MOF-polymer composite
5 Other materials
5.1 Titanium dioxide nanomaterials
5.2 C18
5.3 Mesoporous organosilica
6 Conclusion
Key words: solid-phase microextraction(SPME), new materials, fibers, organic pollutants, environmental analysis

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